Physics – Condensed Matter – Superconductivity
Scientific paper
2001-03-19
Physics
Condensed Matter
Superconductivity
Scientific paper
10.1016/S0921-4534(01)00397-5
Sintered powders and wires of superconducting $MgB_2$ have been fabricated under a variety of conditions in order to determine details of the diffusion of the $Mg$ into $B$ and to study the types of defects that arise during growth. For samples prepared by exposure of boron to $Mg$ vapor at $950^{\circ}C$, the conversion of particles of less than $100\mu m$ size particles to $MgB_2$ is complete in about $2 h$. The lattice parameters of the $MgB_2$ phase determined from X-ray are independent of the starting stoichiometry and the time of reaction. Wire segments of $MgB_2$ with very little porosity have been produced by reacting $141 \mu m$ diameter boron fibers in an atmosphere of excess $Mg$ vapor at $950^{\circ}C$. Defects in the reacted fibers are predominantly the voids left as the boron is converted to $MgB_2$.
Bud'ko Sergey L.
Canfield Paul. C.
Cunningham Charles E.
Finnemore D. K.
Laabs F.
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