Impedance spectroscopic studies of planetary ball-milled lithium titanium phosphate material

Details Impedance spectroscopic studies of planetary ball-milled lithium titanium phosphate material Impedance spectroscopic studies of planetary ball-milled lithium titanium phosphate material

Nov 2009

adsabs.harvard.edu/cgi-bin/nph-data_query?bibcode=2009phyb..404.3539v&link_type=abstract

Physica B: Physics of Condensed Matter, Volume 404, Issue 20, p. 3539-3543.

Physics

Condensed Matter

2

Ionic Conduction, Grain And Twin Boundaries, Nanocrystalline Materials, Powders, Porous Materials

Scientific paper

The ac electrical conductivity properties of LiTi2(PO4)3 (LTP) polycrystalline material in two different crystallite sizes are compared. Micrometer sized LTP is prepared by conventional solid-state reaction. LTP crystallites of 71 nm size are prepared by solid-state reaction of 40 h planetary milled stoichiometric mixture. The XRD and SEM are used as characterization techniques. Electrical properties are studied using impedance spectroscopic technique. Ball-milled LTP shows one order increase in grain-interior conduction compared to microcrystalline LTP at 388 K. The increase in conduction results from decreased crystallite size.

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