Accurate measurement of ^{13}C - ^{15}N distances with solid-state NMR

Details Accurate measurement of ^{13}C - ^{15}N distances with solid-state NMR Accurate measurement of ^{13}C - ^{15}N distances with solid-state NMR

2006-02-18

arxiv.org/abs/cond-mat/0602439v1

J. Chem. Phys. 124, 144508 (2006)

Physics

Condensed Matter

Other Condensed Matter

12 pages

Scientific paper

10.1063/1.2191043

Solid-state NMR technique for measureing distances between hetero-nuclei in static powder samples is described. It is based on a two-dimensional single-echo scheme enhanced with adiabatic cross-polarization. As an example, the results for intra-molecular distances in $\alpha$-crystalline form of glycine are presented. The measured NMR distances ^13 C(2) - ^15 N and ^13 C(1) - ^15 N are 1.496 $\pm$ 0.002 \AA and 2.50 $\pm$ 0.02 \AA, respectively.

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