Waveguide Chirped-Pulse Fourier Transform Microwave Cp-Ftmw Spectrum of Ortho-Fluorotoluene

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Microwave

Scientific paper

The microwave spectrum of o-fluorotoluene has been measured at 0°C from 8.7--18.3 GHz with waveguide chirped-pulse Fourier transform microwave spectroscopy (CP-FTMW). We have extended previous assignments of the lowest energy A- and E-states by Susskind and Mäder and report on preliminary assignments of vibrationally excited states. This molecule also serves as a proof-of-principle for ``coarse" microwave-microwave double resonance (MW-MW DR) measurements, in which we pump all transitions within a relatively broad frequency range (> 50 MHz) simultaneously. Transitions connected to peaks within the bandwidth of the coarse pulse are intensity modulated, revealing approximate connectivities that can be refined by performing ``fine" MW-MW DR measurements. Prospects for using this method to perform automated, time-efficient MW-MW DR on samples with dense spectra and unknown assignments will be discussed.
Susskind, J., J. Chem. Phys. 53, 2492 (1970).
Jacobsen, S., Andresen, U., and Mäder, H., Struct. Chem. 14, 217 (2003).

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