Structural, Vibrational and Mechanical Studies of Hydroxyapatite produced by wet-chemical methods

Details Structural, Vibrational and Mechanical Studies of Hydroxyapatite produced by wet-chemical methods Structural, Vibrational and Mechanical Studies of Hydroxyapatite produced by wet-chemical methods

2004-01-31

arxiv.org/abs/physics/0402002v1

Physics

Chemical Physics

6 figures, submitted to PCCP

Scientific paper

Hydroxyapatite samples were produced by two different wet-chemical methods, and characterized by x-ray diffraction, infrared and compression strength measurements. The x-ray diffraction measurements were simulated using the Rietveld method, and structural data as lattice parameters and average crystallite size were obtained. The infrared spectra showed the presence of CO$_3^{2-}$ ions in all samples, indicating a contamination by these ions. By mixing samples produced by both methods, a bioceramic was obtained and, after sintering, samples with very high compression strengths (26--30 MPa) were obtained.

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