Reaction between Diethyl Peroxide and Nitric Oxide

Details Reaction between Diethyl Peroxide and Nitric Oxide Reaction between Diethyl Peroxide and Nitric Oxide

Oct 1952

adsabs.harvard.edu/cgi-bin/nph-data_query?bibcode=1952natur.170..706m&link_type=abstract

Nature, Volume 170, Issue 4330, pp. 706 (1952).

Physics

1

Scientific paper

IN the hope of trapping the radicals probably produced during the photolysis of diethyl peroxide, the vapour of the latter was mixed with a several-fold excess of nitric oxide in a 3-litre `Pyrex' bulb. The mixture was then passed through a water-cooled helical silica tube surrounding a mercury arc into a trap immersed in `Drikold'. Suspiciously large amounts of ethyl nitrite were found in the trap, and even larger quantities were collected in a blank run without the arc. After the mixture had been stored in the dark for twenty-four hours, spectrophotometric examination showed that a major portion of the peroxide had been converted into nitrite.

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