Electron Paramagnetic Resonance Spectrum of the Acetyl Radical

Details Electron Paramagnetic Resonance Spectrum of the Acetyl Radical Electron Paramagnetic Resonance Spectrum of the Acetyl Radical

Mar 1963

adsabs.harvard.edu/cgi-bin/nph-data_query?bibcode=1963natur.197.1103m&link_type=abstract

Nature, Volume 197, Issue 4872, pp. 1103 (1963).

Physics

1

Scientific paper

THE electron paramagnetic resonance (EPR) spectrum of the acetyl radical, CH3CO, has been detected during and after photolysis of biacetyl at 77° K. Small (100 mg) samples of biacetyl were distilled into thin-walled quartz tubes and degassed. The samples were placed in the V-4546 quartz Dewar accessory of a Varian V-4500 spectrometer, and irradiated under liquid nitrogen with a low-pressure mercury arc.

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