Physics
Scientific paper
Jun 1975
adsabs.harvard.edu/cgi-bin/nph-data_query?bibcode=1975rsci...46..752b&link_type=abstract
Review of Scientific Instruments, Volume 46, Issue 6, pp. 752-756 (1975).
Physics
Scientific paper
A new type of coaxial cylindrical dielectric cell for low frequency measurements (up to 1 MHz), and for high resistance samples was designed using conducting Pyrex glass. The cell also contains a mercury regulator with a temperature control of better than +/-0.02°C. The capacity of the cell is 57.03 pF, with a temperature coefficient between 20° and 120°C = - 6.5×10-3 pF/°C. The lead capacitances (fixed internal lead capacitance associated with the cell = 2.72 pF external lead capacitance of the leads joining the cell with measuring instrument = 0.79 pF) are found to be small. The cell is capable of working up to 350°C with mercury and is expected to work from 250° to 500°C with melts of high conductivity solid electrolytes (like MAg4I5, where M stands for K, Rb, Cs, and NH4, etc.). The dielectric constants of cyclohexane, chlorobenzene, bromobenzene, and carbon tetrachloride, etc., were measured with the help of this cell and the results are in very good agreement with literature values. The frequency variation of the cell has also been recorded.
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