Temperature dependence of oxygen isotope fractionation of CO 2 from magnesite-phosphoric acid reaction

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Scientific paper

New experimental results are reported on oxygen isotope fractionation factors, T , between the 18 O compositions of carbon dioxide liberated by phosphoric acid in the temperature interval of 323 to 373K and that of total oxygen from a natural magnesite (MgCO 3 ). These results are distinctly different from some previously published mutually inconsistent data, and can be expressed as a linear relationship: 10 3 ln T = [{(6.845 ± 0.475)*10 5 }/T 2 ] + (4.22 ± 0.08), where 10 3 ln T refers to fractionation at different temperatures T in Kelvin. Fractionation factors have also been determined at 323 and 368K on a natural calcite. The results on calcite are in excellent agreement with previously published data and can be written as:10 3 ln T = [{(5.608 ± 0.151)*10 5 }/T 2 ] + (3.89 ± 0.08). The combined results on magnesite and calcite yield a computed value of = 1.01117 for dolomite at 298K, assuming equal proportion of 0.5 mole of magnesium and calcium in dolomite, the previously reported experimental values being 1.01109 and 1.01110.

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