Photochemistry of Monochloro Complex of Copper (ii) in Solution by Means of Transient Absorption Time-Resolved Ultrafast Spectroscopy

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The photodissociation mechanism of copper (II) chloro complexes in methanol is studied by means of ultrafast broadband time-resolved deep-UV/UV/vis spectroscopy using [CuII(MeOH)_5 Cl]^+ as a model molecule. Upon 255 nm excitation, the majority of [CuII(MeOH)5Cl]+ dissociate to form chlorine atoms Cl. and penthacoordinate copper(I) solvated complexes [CuI(MeOH)5]+, which is followed by recombination back to the parent molecules. A three body-disscoation in which the nascent [CuI(MeOH)5]+ fragment undergoes a methanol-ligand loss is observed to be of minor importance. The solvent influence on the photoreaction will be discussed.

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