Laser probe 40Ar/39Ar dating studies on sub-milligram whole-rock basalt samples: the age of the Steens Mountain geomagnetic polarity transition (revisited)

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The Steens Mountain geomagnetic polarity transition is arguably the most comprehensively studied geomagnetic field reversal trapped in igneous rocks. Over twenty years ago, this reversal was dated at 15.5 +/- 0.3 Ma by the K-Ar method. We have now tested the feasibility of carrying out 40Ar/39Ar dating on < 1 mg samples of fine-grained whole-rock basalt utilizing a laser probe, i.e. on samples ~ 1000 times smaller than have been traditionally analyzed. Twenty samples taken from lava flows below, within and above the reversal (N/R) in Steens Mountain, Oregon, have been studied by this laser incremental heating technique. Eighteen of these specimens yield acceptable plateau ages with a weighted mean age of 6.2 +/- 0.1 Ma (standard error on the mean). This result is in excellent agreement with the results obtained on two bulk samples of whole-rock basalt that average 16.1 +/- 0.1 Ma. An attempt to confirm these ages by fusion of plagioclase laths taken from a few of the individual lava flows, was hampered by their low K content (0.2-0.3%) our best estimate for the age of six plagioclase laths each < 1 mg weight, is 16.5 +/- 0.5 Ma. We suggest the techniques utilized herein could be extended to carry out dating of basaltic material of age < 1 Ma.

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