The effect of oxidation on the Verwey transition in magnetite

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Crystal Structure, Magnetite, Oxidation, Phase Transformations, Spinel, Transition Temperature, Electrical Resistivity, Rocks, Sediments, Soils

Scientific paper

It has long been believed that magnetic remanence and susceptibility would change markedly at T(V) in the case of coarse grains but only slightly or inappreciably in the case of fine grains. We find on the contrary that remanence changes at T(V) by 50-80 percent in both large and small crystals, if they are stoichiometric. However, minor surface oxidation suppresses the transition, and the fact that fine grains oxidize more readily leads to an apparent size dependence. Our experiments used submicron magnetite cubes with mean sizes of 0.037, 0.076, 0.10 and 0.22 micron which were initially nonstoichiometric. A saturation isothermal remanent magnetization (SIRM) given in a 2.5 T field at 5 K decreased steadily during zero-field warming to 300 K with little or no indication of the Verwey transition. After the oxidized surface of each crystal was reduced to stoichiometric magnetite, the SIRM decreased sharply during warming by 50-80 percent around 110 K. The change in SIRM for the 0.22-micron grains was almost identical to that measured for a 1.5 mm natural magnetite crystal. Thus a 10 exp 12 change in particle volume does not materially affect the remanence transition at T(V) but oxidation to z = 0.3 essentially suppresses the transition.

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